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[0082] (1) Dissolve 150mL of ethanol solution with 2-(2-aminoethoxy)ethanol 2 as the starting material (100mmol, 10.5g), and add di-tert-butyl dicarbonate (100mmol, 23mL) dropwise under ice bath conditions , removed the ice bath, reacted at room temperature for 2h, distilled off the ethanol solvent under reduced pressure

However, persistent side effects may reduce treatment adherence, slowing progress

That translates to roughly 56 lb for someone starting at 231 lb